Abstract
The present study focuses on the development of a new route for the synthesis of pure nickel borate nanoparticles using reverse micellar route. Nickel borate nanoparticles (25 nm) were synthesized from a precursor (obtained by reverse micellar route) containing both nickel and boron (nickel nitrate and sodium borohydride as starting materials). Decomposition of the precursor at a temperature of ∼800 °C yielded pure nickel borate nanoparticles. This was confirmed by powder X-ray diffraction and transmission electron microscopy. These nanoparticles show an antiferromagnetic ordering with Ne{hook above}el temperature of 47 K.
| Original language | English (US) |
|---|---|
| Pages (from-to) | 1002-1005 |
| Number of pages | 4 |
| Journal | Journal of Organometallic Chemistry |
| Volume | 695 |
| Issue number | 7 |
| DOIs | |
| State | Published - Apr 1 2010 |
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All Science Journal Classification (ASJC) codes
- Biochemistry
- Physical and Theoretical Chemistry
- Organic Chemistry
- Inorganic Chemistry
- Materials Chemistry
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A new low temperature methodology to obtain pure nanocrystalline nickel borate. / Menaka, ; Lofland, Samuel; Ramanujachary, Kandalam; Ganguli, Ashok K.
In: Journal of Organometallic Chemistry, Vol. 695, No. 7, 01.04.2010, p. 1002-1005.Research output: Contribution to journal › Article
TY - JOUR
T1 - A new low temperature methodology to obtain pure nanocrystalline nickel borate
AU - Menaka,
AU - Lofland, Samuel
AU - Ramanujachary, Kandalam
AU - Ganguli, Ashok K.
PY - 2010/4/1
Y1 - 2010/4/1
N2 - The present study focuses on the development of a new route for the synthesis of pure nickel borate nanoparticles using reverse micellar route. Nickel borate nanoparticles (25 nm) were synthesized from a precursor (obtained by reverse micellar route) containing both nickel and boron (nickel nitrate and sodium borohydride as starting materials). Decomposition of the precursor at a temperature of ∼800 °C yielded pure nickel borate nanoparticles. This was confirmed by powder X-ray diffraction and transmission electron microscopy. These nanoparticles show an antiferromagnetic ordering with Ne{hook above}el temperature of 47 K.
AB - The present study focuses on the development of a new route for the synthesis of pure nickel borate nanoparticles using reverse micellar route. Nickel borate nanoparticles (25 nm) were synthesized from a precursor (obtained by reverse micellar route) containing both nickel and boron (nickel nitrate and sodium borohydride as starting materials). Decomposition of the precursor at a temperature of ∼800 °C yielded pure nickel borate nanoparticles. This was confirmed by powder X-ray diffraction and transmission electron microscopy. These nanoparticles show an antiferromagnetic ordering with Ne{hook above}el temperature of 47 K.
UR - http://www.scopus.com/inward/record.url?scp=77749330244&partnerID=8YFLogxK
UR - http://www.scopus.com/inward/citedby.url?scp=77749330244&partnerID=8YFLogxK
U2 - 10.1016/j.jorganchem.2009.10.023
DO - 10.1016/j.jorganchem.2009.10.023
M3 - Article
AN - SCOPUS:77749330244
VL - 695
SP - 1002
EP - 1005
JO - Journal of Organometallic Chemistry
JF - Journal of Organometallic Chemistry
SN - 0022-328X
IS - 7
ER -